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Synthesis, Structure, and Reaction of the Tetrahydroxycyclotetrasiloxane, [(i-Pr)(OH)SiO]4
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Citations
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References
1998
Year
X-ray CrystallographyInorganic ChemistryChemical EngineeringEngineeringHeterocyclicNatural SciencesAbstract CisOrganic ChemistryChemistryHeterocycle ChemistryOrganometallic PolymerGood YieldInorganic Synthesis
Abstract cis,cis,cis-1,3,5,7-Tetrahydroxy-1,3,5,7-tetraisopropylcyclotetrasiloxane (1) was synthesized. The X-ray crystallography of 1 revealed that four molecules of 1 and four molecules of water compose a cluster in the lattice. Dehydration of 1 with N,N'-dicyclohexylcarbodiimide (DCC) gave octa(isopropylsilsesquioxane) in good yield.
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