Publication | Closed Access
2,2,4,4,6,6-Hexabenzylcyclotristannatellurane, (Bn<sub>2</sub>SnTe)<sub>3</sub>. Synthesis and Structural Characterization of an Organometallic Single-Source Precursor to Phase-Pure, Polycrystalline SnTe
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References
1999
Year
Structural CharacterizationEngineeringOrganometallic Single-source PrecursorOrganic ChemistryChemistryTitle CompoundInorganic MaterialInorganic CompoundMaterials ScienceInorganic ChemistryOrganometallic PolymerPolycrystalline SnteCrystallographyInorganic SynthesisBiomolecular EngineeringPhase-pure Cubic SnteCoordination ComplexHigh YieldMain Group ChemistrySynthetic Chemistry
The title compound, (Bn2SnTe)3, Bn = CH2C6H5, was prepared in high yield by treating Bn2SnCl2 with (NH4)2Te. Details of the synthesis and characterization (1H, 13C, 119Sn, and 125Te NMR; IR, single-crystal XRD, and elemental analyses) are presented. (Bn2SnTe)3 serves as an efficient single-source precursor to phase-pure cubic SnTe under mild conditions
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