Concepedia

Microwave-assisted Alkylation of p-tert-butylcalix[4]arene Lower Rim: The Effect of Alkyl Halides

Ramil Nugmanov, R. R. Ibragimova, S. Е. Solovieva, A. I. Konovalov

Mendeleev Communications · 2013 · 10 citations · 18 references

DOI

Abstract

Alkylation of p-tert-butylcalix[4]arenes with alkyl bromides or iodides under microwave irradiation affords mostly the corresponding distal disubstituted ethers, whereas in case of alkyl chlorides reasonable yields of monoethers were achieved.

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