Concepedia

An Efficient and Facile Procedure for the Deprotection of 1,1-Diacetates Catalysed by Expansive Graphite

Tong‐Shou Jin, Yanran Ma, Zhan‐Hui Zhang, Tong‐Shuang Li

Synthetic Communications · 1997 · 51 citations · 14 references

DOI

Concepts

Abstract

Abstract A rapid, efficient and high yield method for the deprotection of 1,1-diacetates is described which occurs under catalysis of expansive graphite in refluxing dichloromethane or benzene.

References

14

Protecting groups in organic synthesis. Part 8. Conversion of aldehydes into geminal diacetates

K. S. KOCHHAR, Balkrishna S. Bal, R. P. DESHPANDE et al. · The Journal of Organic Chemistry · 1983 · 231 citations

, , +8

Preparation and spectral properties of benzylidene diacetates

Fillmore Freeman, Elaine Marie Karchefski · Journal of Chemical & Engineering Data · 1977 · 124 citations

, , +8

Phosphorus Trichloride as Catalyst in the Preparation of 1,1-Diacetates from Aldehydes

Jacqueline K. Michie, J. A. MILLER · Synthesis · 1981 · 119 citations

, , +10

Alumina-mediated deacetylation of benzaldehyde diacetates. A simple deprotection method

Rajender S. Varma, Arnab Chatterjee, Manju Varma · Tetrahedron Letters · 1993 · 118 citations

, , +5

An efficient synthesis of diacetates from aldehydes using beta zeolite

Pradeep Kumar, Vishnumurthy R. Hegde, T. P. KUMAR · Tetrahedron Letters · 1995 · 114 citations

, , +13