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Assignment of the 5,6‐Double‐Bond Configuration in Iloprost and Isoiloprost from <sup>13</sup>C‐NMR Shifts Determined by 2D Methods
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1986
Year
Medicinal ChemistryHeterocyclicBiochemistryH ResonancesNatural SciencesChemical BondMolecular BiologySpectra-structure CorrelationOrganic ChemistryH‐nmr MethodsChemistrySolution Nmr SpectroscopyHeterocycle Chemistry5,6‐Double BondNuclear Magnetic Resonance Spectroscopy
Abstract The configurations of the 5,6‐double bond in the carbacyclins iloprost ( 3 ; ( E )) and isoiloprost ( 4 ; ( Z )) are based on a complete assignment of the 13 C and 1 H resonances determined by 1D and 2D 13 C‐NMR and 1 H‐NMR methods.
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