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Identification of the Absolute Configuration of Pectenotoxin-6, a Polyether Macrolide Compound, by NMR Spectroscopic Method Using a Chiral Anisotropic Reagent, Phenylglycine Methyl Ester
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1997
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Macromolecular ChemistryEngineeringNmr SpectroscopyOrganic ChemistryComparative ToxicologyToxicological MechanismBioanalysisToxicologyPolymer ChemistryMicrobial ToxinSynthetic MacromoleculeAbsolute ConfigurationPhenylglycine Methyl EsterBiochemistryPolymer AnalysisExperimental ToxicologyPharmacologyBiomolecular EngineeringChiral Anisotropic ReagentPolymer ScienceMedicine
The absolute configuration of pectenotoxin-6 (4, PTX6), found in association with diarrhetic shellfish poisoning, was identified by NMR spectroscopy using a chiral anisotropic reagent, phenylglycine methyl ester (PGME), which was condensed with a carboxyl group of 4.