Chinese Journal of Chemistry · 2004 · 13 citations · 13 references
Natural SciencesChemistryMaterials ScienceElectrochemical EngineeringElectrochemistryInorganic ChemistryCathode MaterialsElectroanalytical ChemistryElectrochemical CellsElectrochemical Energy ConversionElectrode MaterialsElectrode-electrolyte InterfacesCo2 ElectrolysisCobalt OxidesElectrochemical BehaviorElectrochemical MeasurementsElectrochemical MechanismsElectrochemical ReductionNanocrystalline MaterialsVoltammetry
Abstract Electrolytic fixation of CO 2 was investigated by electrocarboxylation of organic halides (a), and four esters (I, II, III, IV) were obtained in moderate yields. Electrochemical reduction esterifications of RX in the presence of CO 2 were carried out on nanocrystalline TiO 2 ‐Pt electrode. The electrochemical behavior of RX in the presence of CO 2 was investigated by the technique of cyclic voltammetry, and the probable reaction mechanism was proposed.
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