Physical review. B, Condensed matter · 1998 · 51 citations · 11 references
Natural SciencesMaterials SciencePhysicsCondensed Matter PhysicsElectromagnetismMagnetic MaterialsFerromagnetic MaterialsFerromagnetismMagnetic Properties Of SolidsMagnetism In SolidsMagnetization ProcessesPhase TransitionsHysteresisHysteresis BehaviorHysteresis LoopsInversion SymmetryMagnetic HysteresisMemory EffectsTime Reversal SymmetryTime-reversal Symmetry Breaking
We have used ballistic Hall micromagnetometry to study the magnetization of individual submicrometer nickel disks (80 nm high, $0.1--1.0\ensuremath{\mu}\mathrm{m}$ diameter). At low temperatures, hysteresis loops of the disks no longer show inversion symmetry in a magnetic field, as if the time reversal symmetry were broken. Furthermore, the magnetization of the smallest disks can be ``frozen'' in two possible states that are characterized by hysteresis loops which are each other's inverse. At temperatures below 19.5 K a magnetic field as high as 2 T cannot switch between the states, proving that it is extremely difficult to fully polarize a small ferromagnetic particle. On the other hand, at slightly higher temperatures (only $T>19.8 \mathrm{K}),$ a field as low as 0.1 T appears to be enough to fully polarize the disks. We attribute this extraordinary behavior to the glass-liquid transition experienced by spins at the particle surface.
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