Journal of the Chemical Society Perkin Transactions 2 · 2000 · 15 citations · 10 references
EngineeringChemical EngineeringChemistryPharmaceutical FormulationReaction EngineeringSupramolecular ChemistryEmulsion FormationEmulsion FormulationLiquid ChromatographySurfactantsArginine-based AgentsConcentrated EmulsionsDispersed Phase Volume FractionSurfactant FormulationSurfactant SolutionsSurfactant SynthesisVolume Fraction EffectsWater-in-oil Emulsions
Synthesis of the cationic surfactant Nα-lauroylarginine methyl ester hydrochloride (LAM) has been carried out using highly concentrated water-in-oil emulsions as new reaction media. The influence of reaction time, ArgOMe-dodecanoic acid molar ratio, temperature and the volume fraction of the dispersed phase on reaction yield has been studied. A new HPLC analysis procedure and a MPLC purification for LAM is described.
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A New Method of Forming Peptide Bonds
John C. Sheehan, George P. Hess · Journal of the American Chemical Society · 1955 · 1.3K citations
The formation of gel-emulsions in a water/nonionic surfactant/oil system
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