Publication | Closed Access
Expeditious Microwave-Assisted Thionation with the System PSCl<sub>3</sub>/H<sub>2</sub>O/Et<sub>3</sub>N under Solvent-Free Condition
46
Citations
10
References
2008
Year
Chemical EngineeringEngineeringExpeditious Microwave-assisted ThionationRadiofrequency HeatingGreen ChemistryChemical DerivativeThiocarbonyl CompoundsOrganic ChemistryNovel Thionation ProtocolMicrowave IrradiationChemistryHeterocycle ChemistryMicrowave SynthesisSynthetic ChemistryEnantioselective Synthesis
A novel thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
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