Fundamentals of ion-beam-assisted deposition. II. Absolute calibration of ion and evaporant fluxes

G. K. Hubler, D. Van Vechten, E. P. Donovan, C.A. Carosella

Journal of Vacuum Science & Technology A Vacuum Surfaces and Films · 1990 · 57 citations · 0 references

Concepts

Abstract

A method is given to obtain an absolute calibration of the ion and evaporant fluxes in an ion-beam-assisted deposition system based upon a Kaufman ion source and an electron beam vapor source. The nitrogen-ion silicon-vapor material system is used for the calibration; Rutherford backscattering is used for measurement of composition and thickness of Si1−x Nx films deposited on C and Si substrates. It is shown that quantitative predictions of the ion-to-atom impingement ratio, film composition, and film thickness can be obtained when sputtering, reflection, charge exchange neutralization of the ions, and species content of the nitrogen beam are considered.