Acta Crystallographica Section B Structural Science · 1992 · 26 citations · 0 references
Natural SciencesChemistryMaterials ScienceCrystal StructureInorganic ChemistryMineralogyCoordination ChemistryCrystal ChemistryCrystal SystemsMetal OxidesX-ray CrystallographyX-ray DiffractionAlkali Metal ChemistryCoordination Number In Ionic CrystalsOctahedral CoordinationPerchlorate SaltsRay StructureX-ray ChemistryX-ray Structure Determination
(C 12 H 24 O 6 )K + .ClO 4 - cristallise dans P2 1 /n avec, a 295 K, a = 8,299, b = 15,012 et c = 15,267 A, β = 103,15 °; affinement jusqua R = 0,042. A 20 K, a = 8,251, b = 14,757 et c = 15,057 A, β = 105,33 °; affinement jusqu'a R = 0,027. L'ion potassium est coordine aux six oxygene de l'ether et aux deux anions perchlorate.