Concepedia

Solid State Acetylation with Acetylimidazole: Selective Protection of Primary Alcohols and Phenols

Hisahiro Hagiwara, Kimie Morohashi, Toshio Suzuki, Masayoshi Ando, Isao Yamamoto, Michiharu Kato

Synthetic Communications · 1998 · 30 citations · 16 references

DOI

Concepts

Abstract

Abstract Primary alcohols and phenols have been acetylated with acetylimidazole by the solid state reaction, grinding both substrates with a pestle in a mortar.

References

16

Protective groups in organic synthesis

Philip Hodge · Polymer · 1992 · 2.2K citations

, , +8

Scandium Trifluoromethanesulfonate as an Extremely Active Lewis Acid Catalyst in Acylation of Alcohols with Acid Anhydrides and Mixed Anhydrides

Kazuaki Ishihara, Manabu Kubota, Hideki Kurihara et al. · The Journal of Organic Chemistry · 1996 · 429 citations

, , +16

Chemical synthesis of 2-acetamido-2-deoxy-4-O-(.alpha.-L-fucopyranosyl)-3-O-(.beta.-D-galactopyranosyl)-D-glucose. Lewis a blood-group antigenic determinant

R. U. Lemieux, Hugues Driguez · Journal of the American Chemical Society · 1975 · 222 citations

, , +11

Tributylphosphine-catalyzed acylations of alcohols: scope and related reactions

Edwin Vedējs, Nancy Bennett, Lisa Marie Conn et al. · The Journal of Organic Chemistry · 1993 · 203 citations

, , +6

Total synthesis of prostaglandin F2.alpha. by chirality transfer from D-glucose

Gilbert Stork, Takashi Takahashi, Isao Kawamoto et al. · Journal of the American Chemical Society · 1978 · 111 citations

, , +10