Improved thermomechanical properties of carbon fiber reinforced epoxy composite using amino functionalized XDCNT

Abstract

ABSTRACT Carbon fiber‐reinforced epoxy composites (CFEC) are fabricated infusing up to 0.40 wt % amino‐functionalized XD‐grade carbon nanotubes (XDCNT) using the compression molding process. Interlaminar shear strength (ILSS) and thermomechanical properties of these composites are evaluated through short beam shear and dynamic–mechanical thermal analysis tests. XDCNTs are infused into Epon 862 resin using a mechanical stirrer followed by sonication. After the sonication, the mixture was placed in a three roll milling processor for three successive cycles at 140 rpm for uniform dispersion of CNTs. Epikure W curing agent was then added to the resin using a high‐speed mechanical stirrer. Finally, the fiber was reinforced with the modified resin using the compressive mold. ILSS was observed to increase by 22% at 0.3 wt % XDCNT loading. Thermal properties, including storage modulus, glass transition temperature, and crosslink density demonstrated linear enhancement up to the 0.3 wt % XDCNT loading. Scanning electron microscopy revealed better interfacial bonding in the CNT‐loaded CFEC. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131 , 40709.