Concepedia

A CONVENIENT PREPARATIVE METHOD OF CARBOHYDRATE PHOSPHATES WITH BUTYLLITHIUM AND PHOSPHOROCHLORIDATE

Masaru Inage, H. CHAKI, Shoichi Kusumoto, Tetsuo Shiba

Chemistry Letters · 1982 · 71 citations · 5 references

DOI

Concepts

Abstract

Abstract α-Glycosyl phosphates and 4-phosphates of N-acylglucosamine derivatives were prepared in high yields via the reaction of corresponding O-lithium salts with dibenzyl or diphenyl phosphorochloridate at low temperature.

References

5

α- and β-d-glucopyranosyl phosphates from 0-α-D-glucoypyranosyl trichloroacetimidates

Richard R. Schmidt, Michael Stumpp, Josef Michel · Tetrahedron Letters · 1982 · 68 citations

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The synthesis of P1-2-acetamido-4-O-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-2-deoxy-α-d-glucopyranosyl P2-dolichyl pyrophosphate, (P1-di-N-acetyl-α-chitobiosyl P2-dolichyl pyrophosphate)

Christopher D. Warren, Annete Herscovics, Roger W. Jeanloz · Carbohydrate Research · 1978 · 38 citations

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Chemical synthesis of phosphorylated fundamental structure of lipid a

Masaru Inage, H. CHAKI, Shoichi Kusumoto et al. · Tetrahedron Letters · 1981 · 38 citations

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Stereochemical control in the acylation of 2,3,4,6-tetra-O-benzyl-D-glucopyranose. A route to 1-O-acyl-.alpha.- and -.beta.-D-glucopyranoses

Philip E. Pfeffer, Edward S. Rothman, Gordon G. Moore · The Journal of Organic Chemistry · 1976 · 31 citations

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Use of O-thallium(I) salts in the synthesis of phosphate, sulfite, and related ester derivatives of carbohydrates

Alessandro Granata, Arthur S. Perlin · Carbohydrate Research · 1981 · 30 citations

, , +10