Synthetic Communications · 2013 · 50 citations · 25 references
Chemical EngineeringAmino-functionalized Mcm-41Catalytic AmountEngineeringNatural SciencesDiversity-oriented SynthesisCatalytic SynthesisSustainable SynthesisOrganic ChemistryCatalysisChemistryAqueous MediaSynthesis MethodSynthetic ChemistryBiomolecular EngineeringEfficient One-pot Method
Abstract A convenient and efficient one-pot method for the synthesis of 2-amino-tetrahydro-4H-chromene and 2-amino-4H-benzo[h]-chromene derivatives has been developed using a catalytic amount of amino-functionalized MCM-41 in aqueous medium. This efficient technique has the advantages of giving 4H-tetrahydro-chromene and 4H-benzo[h]chromene building blocks using a reusable catalyst in good to excellent yields, to be completed in short reaction times with a simple product isolation procedure.
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Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism
Charles T. Kresge, M. E. Leonowicz, Wiesław J. Roth et al. · Nature · 1992 · 16.1K citations
Susumi Hatakeyama, Noriko Ochi, Hirotoshi Numata et al. · Journal of the Chemical Society Chemical Communications · 1988 · 293 citations
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