Publication | Closed Access
Simplification of the Mitsunobu Reaction. Di-<i>p</i>-chlorobenzyl Azodicarboxylate: A New Azodicarboxylate
85
Citations
6
References
2006
Year
Cross-coupling ReactionEngineeringMitsunobu ReactionBiochemistryNatural SciencesDi-p-chlorobenzyl AzodicarboxylateOrganic ChemistryOrganometallic CatalysisSeparable Hydrazine ByproductChemistryHeterocycle ChemistryHalogenationSynthetic ChemistryBiomolecular EngineeringMitsunobu Couplings
Di-p-chlorobenzyl azodicarboxylate (DCAD) is introduced as a novel, stable, solid alternative to DEAD and DIAD for a variety of Mitsunobu couplings. DCAD/Ph(3)P-mediated reactions in CH(2)Cl(2) generate a readily separable hydrazine byproduct. [reaction: see text]
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