Review of Scientific Instruments · 2015 · 133 citations · 14 references
Natural SciencesElectrical EngineeringMicrowave EngineeringSpectroscopic AnalysisSpectroscopyDynamic Nuclear PolarizationMagnetic Resonance SpectroscopyMicrowave MeasurementsMicrowave SpectroscopyNuclear SpectroscopyRadio SpectroscopyCoolant Temperature ControlExperimental DiagnosticsFrequency TuningGyrotron Microwave SourcesMaximum Available PowerMillimeter-wave SpectroscopyRadio-frequency DevicesSpectroscopic Characterization
A 263 GHz continuous-wave (CW) gyrotron was developed at the IAP RAS for future applications as a microwave power source in Dynamic Nuclear Polarization / Nuclear magnetic resonance (DNP/NMR) spectrometers. A new experimental facility with a computerized control was built to test this and subsequent gyrotrons. We obtained the maximum CW power up to 1 kW in the 15 kV/0.4 A operation regime. The power about 10 W, which is sufficient for many spectroscopic applications, was realized in the low current 14 kV/0.02 A regime. The possibility of frequency tuning by variation of the coolant temperature about 4 MHz/1 °C was demonstrated. The spectral width of the gyrotron radiation was about 10(-6).
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Natural Sciences, Chemistry, Physics +13