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Separation of aldose enantiomers by gas-liquid chromatography.
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1986
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Bioorganic ChemistryGas-liquid ChromatographyAldose EnantiomersOrganic ChemistryMedicinal ChemistryGas ChromatographyAnalytical ChemistryLiquid ChromatographyStereoselective SynthesisSe-30 Capillary ColumnL-cysteine Methyl EsterChromatographyBiochemistryChromatographic AnalysisNatural Product SynthesisPharmacologyAsymmetric CatalysisEnantioselective SynthesisNatural SciencesMedicineDrug Analysis
Pairs of enantiomers of nine aldoses were separated on gas-liquid chromatography equipped with an SE-30 capillary column as trimethylsilyl ethers after conversion of the aldoses to methyl 2-(polyhydroxyalkyl)-thiazolidine-(4R)-carboxylates using the reaction with L-cysteine methyl ester.